Table of Contents
Introduction
Sample and Instrumentation
Test Method
Results and Discussion
Conclusion
About Keysight Technologies
Introduction
In a number of materials, the plastic stress that can be sustained depends on strain rate through a powerlaw relationship: higher stresses are sustained with higher strain rates and vice versa. In a uniaxial tensile configuration, this relationship between plastic stress, σ, and strain rate,ε•u, can be expressed via the following equations:

Eq. 1 

Eq. 2 

Eq. 3 
where B* is a constant and m is the strainrate sensitivity (SRS), which is always greater than or equal to zero. For materials showing negligible strainrate sensitivity, m is near zero, making σ a constant. Materials with greater strainrate sensitivity have greater values of m.
By performing a series of indentations, Lucas and Oliver showed that the strainrate sensitivity, m, could be evaluated with each indentation performed using a different strain rate. This approach is challenging since indentations at small strain rates take so long that the results can easily be dominated by thermal drift.
The protocol proposed by Maier et al. has several practical advantages. First, the testing time and thermal drift are minimized by using fast strain rates when the applied force is small and slow strain rates when the applied force is large. The protocol suggested by Maier et al. examines the largest strain rate at the beginning of the test and examines progressively smaller strain rates as the applied force increases.
Both thermal drift and testing time are minimized this way. The protocol of Maier et al. has been implemented in a new Keysight NanoSuite test method. The second benefit of the Maier protocol is that since all strain rates of interest are examined in every test, it is possible to map the spatial distribution of strainrate sensitivity.
Sample and Instrumentation
The sample tested in this work was a NIST standard reference material (SRM) for Vickers hardness. The sample is a 1.35cm square test block of electrodeposited bright nickel, approximately 750µm thick, on an AISI 1010 steel substrate, mounted and highly polished in a thermosetting epoxy. The sample has a smooth surface, a small grain size and is resistant to corrosion and tarnish.
A Keysight NanoIndenter G200 system with a Berkovich indenter was used for all testing. In order to achieve hardness and elastic modulus as a continuous function of penetration depth, Keysight’s Continuous Stiffness Measurement (CSM) option was also used.
Test Method
Using the test method “GSeries XP CSM StrainRate Sensitivity”, twelve indentation tests were performed. Table 1 summarizes testing inputs. This test method enables the user to prescribe a penetration that must be achieved prior to strainrate cycling (Displacement, Initial).
Table 1. Summary of inputs used to measure the strainrate sensitivity of a Ni Vickers SRM by the method “GSeries XP CSM StrainRate Sensitivity.”
On achieving initial penetration, the method prescribes cycling between a test strain rate and a base strain rate. The test strain rate is executed in the first part of the cycle; the base strain rate is executed in the second part of the cycle. Figure 1 shows the strainrate history for each indentation test on the Ni SRM.
Figure 1. Strainrate cycling imposed on the test sample. In the first part of the cycle, the test strain rate is imposed. In the second part of the cycle, the base strain rate is imposed.
Results and Discussion
The most important results are summarized in Table 2. A survey of strainratesensitivity values measured by others for finegrained Ni is shown in Table 3.
Table 2. Summary of results.
Table 3. Survey of SRS (m) values measured by others on finegrained Ni.
The continuous elastic modulus during strainrate cycling for one typical test is shown in Figure 2. As expected, the modulus did not change significantly during strainrate cycling. For each cycle modulus is reported by averaging the continuous measurements that fall within 80–90% of the displacement range for the basestrainrate segment of the cycle. These measurements are plotted as green data points in Figure 2.
Figure 2. Modulus during strainrate cycling for one typical test. As expected, modulus is not sensitive to strain rate.
The modulus value reported for each test in Table 2 is the average of the three cyclelevel results for that test. The average over all tests, 229GPa, is 15% higher than the nominal value of 200GPa for pure nickel.
One can use finiteelement simulations of indentations into a material with nickellike properties for further investigations, since finiteelement simulations allow a comparison between contact area determined by the OliverPharr model and contact area determined from the finiteelement mesh.
Figure 3 shows the continuous hardness measured during strainrate cycling for a typical test. For each test strain rate, the hardness values within 80–90% of the displacement range for the segment are averaged to report a single value of hardness; data within this range for each cycle are plotted as black symbols in Figure 3.
Figure 3. Hardness during strainrate cycling. Sensitivity to strain rate is evident. Black symbols denote data used to calculate the hardness for each test strain rate. Green symbols denote data used to calculate the hardness for each base strain rate.
Figure 4 shows ln(H) vs. ln(ε•) for all 12 tests. The linearity of these results supports the hypothesis that this material is well described by Equation 2.
Figure 4. Plot of ln(H) vs. ln(ε•) for each of 12 tests. Slope of ln(H) in respect to ln(ε•) for each test gives the strainrate sensitivity, m, for that test. Linearity of these data demonstrates that strainrate sensitivity for this material is well modeled by Eq. 2.
For all 12 tests, Figure 5 shows hardness associated with the base strain rate for each cycle.
Figure 5. Hardness measured during the basestrainrate segment of each cycle. Lack of any trend with cycle number demonstrates that the same hardness is measured when the same strain rate is applied, despite increasing penetration.
Conclusion
An experimentally robust test method has been implemented in Keysight NanoSuite for measuring strainrate sensitivity via instrumented indentation. The method overcomes the challenges associated with long testing times by imposing small strain rates only when the applied force is large.
With this method, the strainrate sensitivity of a sample of nickel sold by NIST as a Vickers SRM was measured to be m = 0.021. This value is in good agreement with values obtained by others on similar materials using both instrumented indentation and uniaxial creep testing.
About Keysight Technologies
Keysight is a global electronic measurement technology and market leader helping to transform its customers' measurement experience through innovation in wireless, modular, and software solutions. Keysight provides electronic measurement instruments and systems and related software, software design tools and services used in the design, development, manufacture, installation, deployment and operation of electronic equipment. Information about Keysight is available at www.keysight.com.
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